By Boschke F.L.
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Extra so than any of the opposite significant teams of components within the periodic desk, the transition metals have formed human heritage and feature been the workhorses of undefined. the invention of steel copper ended the Stone Age and ushered within the Bronze Age. Alloys of iron (especially metal) later took over, and the Iron Age changed the Bronze Age.
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54 7. Reactions w i t h Thioethers . . . . . . . . . . . . . . . . . . . . 58 8. Reactions w i t h Aliphatic E t h e r s . . . . . . . . . . . . . . . . . . 9. The R e a c t i o n of T e t r a f l u o r o b e n z y n e w i t h N , N - D i m e t h y l a n i l i n e 59 ....... 60 10. 1]diene . . . 62 11. R e a c t i o n s w i t h F i v e - M e m b e r e d :Ring Dienes . . . . . . . . . . . . 63 12. Reactions w i t h Steroidal Dienes a n d Trienes .
140~ Scate factor 3 Sweep rate 32 Sans. A ~, 9 . 5 Fig. 2. const. IS Teml:z+180~ Scale factor 3 Sweep rate 32 - --Sans. const. +200~ Scale factor 3 Sweep rate 32 Sans. censt. s Fig. 3. +200~ Scare factor 6 Sweep rate 16 Sens. 4. const. 04S 1 0 I 2 3 /, 5 6 ? 0 10 20 30 Z,O 50 60 70 Fig. 4. (Scote 6} 90 100 100Units (38) at 200 ~ for the methyl protons s0L Evidently the increase in the carbon to silicon bond length, compared to the analogous carbon to carbon bond-length results in the reduction of the steric effect.
In the case of the pyrolysis of tetrachlorophthalic anhydride some hexachlorobenzene is also formed, while the pyrolysis of tetrabromophthalic anhydride results in the formation of hexabromobenzene but no octabromobiphenylene. The disproportionation of tetrabromobenzyne to form carbon and bromine is a function of the high temperature involved and, as we shall see later, both tetrabromo- and tetraiodo-benzyne behave normally in solution. Octafluorobiphenylene (15) has been obtained recently, along with octafluorofiuorenone (16), by the pyrolysis of silver tetrafluorophthalate as).
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