By Robert M. Silverstein

This publication is characterised by way of its problem-solving procedure with wide reference charts and tables. First released in 1962, this used to be the 1st e-book at the identity of natural compounds utilizing spectroscopy. Now thought of a vintage, it may be came across at the shelf of each natural Chemist. the major energy of this article is the huge set of real-data difficulties in Chapters eight and nine. Even specialist chemists use those spectra as reference information. Spectrometric identity of natural Compounds is written by means of and for natural chemists, and emphasizes the synergistic impact because of the interaction of the spectra.

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3 and 4 are enantiotopic. O 2 HO 1 3 4 5 6 Hexanoic acid T One spin system. 2, 3, 4, and 5 are enantiotopic. HO 1 Cl 2 3 Cl 3' 4 2,6-Dichlorophenol U One spin system. 3 and 3’ are CSE but not magnetically equivalent. HO 5 1 2 6 3 3' 4 2,6-Dimethylphenol V One spin system. 3 and 3’ are CSE but not magnetically equivalent. 5 and 6 are CSE. O 1 6 5 4 2 3 2-Cyclohexen-1-one W One spin system. 4, 5, and 6 are enantiotopic. 2 Note -- These are not close to observed values, but are the only answer from given tables.

3 O - 2 1 N+ 4 Cl O 3' 2' 1-Chloro-4-Nitrobenzene P One spin system. 2 and 2’ are CSE but not magnetically equivalent as are 3 and 3’. O HO 1 2 3 4 5 6 7-Bromo Heptanoic Acid Q One spin system. 2, 3, 4, 5, 6, and 7 are enantiotopic. 6 26 6 2 HO 1 3 4 5 5-Hexyn-1-ol R One spin system with long range coupling. 1, 2, 3, and 4 are enantiotopic. 8 O 5 3 2 4 6 7 6-Methyl-5-hepten-2-one 1 S At 2 spins systems (7 and 8 probably have long range coupling). 3 and 4 are enantiotopic. O 2 HO 1 3 4 5 6 Hexanoic acid T One spin system.

6 24 2 H2N 1 4 3 Butylamine G Pople Notation – A3G2M2X2One spin system. 1, 2, and 3 are enantiotopic. 1 OH 2 3 Propargyl alcohol H One spin system with long range coupling. Protons on 2 enantiotopic. O - O N+ 1 3 2 1-Nitropropane I Pople Notation -- A3M2X2. 1 and 2 are enantiotopic. 3 4 3' 2 1 5 6 OH O 2' 2-Phenoxylethanol J Two spins systems; Pople Notation -- AA’MM’X and A2X2. 2 and 2’are CSE but not magnetically equivalent as are 3 and 3’. 5 and 6 are enantiotopic. 6 2 5 O 3 1 4 2' 3' Phenetole K Two spins systems; Pople Notation -- AA’MM’X and A3X2.

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